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51.
Isolation,purification, and antioxidant activities of polysaccharides from Ziziphus Jujuba cv. Muzao
In the present study, crude polysaccharides from Ziziphus Jujuba cv. Muzao were isolated and purified using DEAE cellulose-52 and Sephadex G-100 size-exclusion chromatography; four fractions were collected, namely GZMP-1, GZMP-2, GZMP-3, and GZMP-4. The molecular weights of these four fractions were measured to be 111.2, 95.1, 84.2, and 571.4 kDa, respectively, using high-performance gel permeation chromatography. Gas chromatography analysis of the monosaccharide composition confirmed that GZMP-1 was composed of rhamnose, arabinose, glucose, and galactose. Rhamnose, arabinose, and galactose were the main components present in GZMP-2 and GZMP-3, whereas GZMP-4 was composed of only rhamnose and arabinose. Scanning electron microscopy showed relatively smooth surfaces for GZMP-1 and GZMP-4, whereas GZMP-2 and GZMP-3 had more folds on their surfaces. Fourier transform infrared spectroscopy analyses indicated that GZMP-1 and ZMP mainly had α-type glycosidic linkages. The in vitro antioxidant activities of the polysaccharides revealed that jujube polysaccharides exhibit remarkable antioxidant activity, and can scavenge DPPH radical and OH radical in a concentration-dependent manner. The results of this work suggest that polysaccharides from Z. Jujuba cv. Muzao have potential to be used as functional food and in the development of natural antioxidant drug carriers. 相似文献
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55.
Haiyi Peng Haishen Ren Mingzhao Dang Yi Zhang Xiaogang Yao Huixing Lin 《Ceramics International》2018,44(6):6527-6532
Ca0.9La0.067TiO3 (abbreviated as CLT) ceramics doped with different amount of Al2O3 were prepared via the solid state reaction method. The anti-reduction mechanism of Ti4+ in CLT ceramics was carefully investigated. X-ray diffraction (XRD) was used to analyze the phase composition and lattice structure. Meanwhile, the Rietveld method was taken to calculate the lattice parameters. X-ray photoelectron spectroscopy (XPS) was employed to study the valence variation of Ti ions in CLT ceramics without and with Al2O3. The results showed that Al3+ substituted for Ti4+ to form solid solution and the solid solubility limit of Al3+ is near 1.11 mol%. Furthermore, the reduction of Ti4+ in CLT ceramics was restrained by acceptor doping process and the Q × f values of CLT ceramics were improved significantly. The CLT ceramic doped with 1.11 mol% Al2O3 exhibited good microwave dielectric properties: εr = 141, Q × f = 6848 GHz, τf = 576 ppm/°C. 相似文献
56.
Wahab Ali Khan Masood Sadiq Butt Imran Pasha Muhammad Saeed Iqra Yasmin Maratab Ali Muhammad Azam Muhammad Shahroz Khan 《Journal of texture studies》2020,51(6):955-967
Vitamin D lost its functionality during processing and storage, thus, encapsulation with proteins is desirable to preserve bioactivity. The aim of the current study was to develop encapsulated vitamin D fortified mayonnaise (VDFM) using whey protein isolates (WPI) and soy protein isolates (SPI) as encapsulating materials in three different formulations, that is, 10% WPI, 10% SPI, and 5/5% WPI/SPI. Increased shear stress decreased the apparent viscosity along with significant effects on the loss modulus of VDFM. WPI encapsulates showed better results as compared to SPI. WPI based VDFM (M1) depicted the best results in terms of size and dispersion uniformity of oil droplets. Hue angle and total change differed significantly among treatments. The highest value for overall acceptability was acquired by M3 (5:5%WPI:SPI-encapsulates) thus proceed for in vivo trials. Serum vitamin D level was significantly higher in the encapsulated VDFM rat group (58.14 ± 6.29 nmol/L) than the control (37.80 ± 4.98 nmol/L). Conclusively, WPI and SPI encapsulates have the potential to improve the stability and bioavailability of vitamin D. 相似文献
57.
原位胶结充填体质量评价通常采用单轴抗压强度作为表征指标,由于在现场工程中无法快速、准确获取充填体的强度值,因此需要建立一种参数易于获取且准确的原位胶结充填体强度预测模型。基于胶结充填体物理力学参数的内在联系,从量纲平衡的角度探索了胶结充填体单轴抗压强度与P波模量的关系。根据C矿和I矿两种原位胶结充填体的密度、P波速度及取芯强度的测试数据,采用线性拟合的方法获得了基于P波模量的原位胶结充填体强度预测模型。通过对C矿和I矿的强度预测模型拟合效果分析可知,P波模量与取芯强度呈正相关性,且拟合效果较好,证明原位胶结充填体强度预测模型精度高,具有很强的实用性。 相似文献
58.
在对沁水盆地赵庄矿煤层气开发地质、煤层气生产井资料深入研究的基础上,分析、总结了区内煤层气直井低产原因,并据此提出了区内地面抽采后续开发方向。研究认为:3号煤层气含量偏低、含气饱和度低、临储比低,致使排采阶段气含量可降幅度低,是其低产的宏观表征;3号煤储层不匹配孔级,较差连通性,即微、小孔为主,中孔次之,大孔不发育,微裂隙连通性差,致使扩散缓慢、影响储层改造和抽采效果,是其低产的微观表征;3号煤层远高于顶底板塑性及相近的水平应力,进一步造成改造缝长受限,泄流面积不足。因此,建议区内后续地面抽采方式应以增大泄流面积开发方式为主。 相似文献
59.
针对65号航空冷却液在过滤循环中出现泡沫较多的现象,对65号航空冷却液泡沫倾向性进行探究。按照石化行业标准《发动机冷却液泡沫倾向测定法(SH /T 0066-2002)》,利用冷却液泡沫倾向测定仪来评价65号航空冷却液泡沫倾向性,并进行水乙二醇溶液对照试验。结果表明,航空冷却液在低温和循环时间较长的情况下,其泡沫倾向性较大,而随着温度的升高和循环时间的缩短,泡沫倾向性有一定程度的改善;并且通过水乙二醇对照试验可知,冷却液的基础液泡沫倾向性较小。航空冷却液在过滤循环中出现的泡沫问题,是加入的添加剂所引起的。 相似文献
60.
Prof. Chiara Brullo Dr. Federica Rapetti Prof. Silvana Alfei Dr. Irena Maric Dr. Francesca Rizzelli Dr. Marina Mapelli Dr. Camillo Rosano Dr. Maurizio Viale Prof. Olga Bruno 《ChemMedChem》2020,15(11):961-969
Even though immunotherapy has radically changed the search for anticancer therapies, there are still many different pathways that are open to intervention with traditional small molecules. To expand our investigation in the anticancer field, we report here a new series of compounds in which our previous pyrazole and imidazopyrazole scaffolds are linked to a differently decorated phenyl ring through an acylhydrazone linker. Preliminary tests on the library were performed at the National Cancer Institute (USA) against the full NCI 60 cell panel. The best compounds among the imidazopyrazole series were then tested by immunofluorescence staining for their inhibition of cell proliferation, apoptosis induction, and their effect on the cell cycle and on microtubules. Two compounds, in particular 4-benzyloxy-3-methoxybenzyliden imidazopyrazole-7-carbohydrazide showed good growth inhibition, with IC50 values in the low-micromolar range, and induced apoptosis. Both compounds altered the cell-cycle phases with the appearance of polyploid cells. Immunofluorescence analysis evidenced microtubules alterations; tubulin polymerization assays and docking studies suggested the tubulin system to be the possible, although not exclusive, target of the new acylhydrazone series reported here. 相似文献